王鲲鹏   Associate professor

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4-硝基苯甲酸甲酯合成工艺研究

Release time:2024-12-23  Hits:

  • Key Words:4-硝基苯甲酸甲酯;4-硝基苯甲酸;碳酸二甲酯;酯化反应;工艺优化;绿色合成
  • Abstract:对以4-硝基苯甲酸为原料，合成4-硝基苯甲酸甲酯的生产路线进行了工艺优化。考察了催化剂、溶剂、温度、母液套用次数对反应的影响。优化的工艺条件为：发烟硫酸为催化剂，碳酸二甲酯为溶剂，回流温度反应10 h,母液套用5次，在此条件下，收率可达到94.7%。
  • Volume:v.61
  • Issue:01
  • Translation or Not:no
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