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Effects of annealing processes on the crystallization and magnetic properties of nickel ferrite thin films

发布时间:2021-03-15点击次数:

  • 关键字:ORIENTED GROWTH; SOLUTION DEPOSITION; NIFE2O4; TEMPERATURE
  • 摘要:Magnetic nickel ferrite (NFO), NiFe2O4, thin films were fabricated using the chemical solution deposition method on (100)-oriented silicon substrates. The effects of an annealing process on the crystallization and magnetic properties of NFO thin films were investigated. Two annealing methods were used, namely layer-by-layer multiple rapid-annealing process and single slow-annealing process. The results showed that the appropriate pyrolysis temperatures range from 400 to 500 degrees C. NFO thin films crystallized well when they were annealed at 750 degrees C or above. The NFO thin films fabricated using the single slow-annealing process (NFO-S) show better crystallinity compared to the films fabricated using the layer-by-layer multiple rapid-annealing process (NFO-R) when the annealing temperatures were low. NFO-R thin films show preferred (400) orientation growth and the relative intensity of the (400) peak raises with the annealing heating rate. Fine magnetic hysteresis loops and good magnetic properties were observed in both NFO-S and NFO-R thin films. A saturation magnetization of 277 emu cm(-3)was derived for the NFO-S thin films, compared to a 230 emu cm(-3)for the NFO-R thin films, which is a very high value compared with former reported values for NFO thin films.
  • 卷号:43
  • 期号:1
  • 是否译文:否
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  • 毕业院校:中国科学院上海硅酸盐研究所
  • 学历:博士研究生
  • 学科: 材料物理与化学;
    材料学

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