摘要:NaYF4:Yb3+/Er3+ nanocrystals were prepared using a hydrothermal method. The products were characterized by XRD, SEM, TEM, HRTEM, and photoluminescence (FL). The XRD results indicated that the sample's phase transformed from cubic to hexagonal when EDTA was added at low reaction temperatures. The SEM results revealed that the products were transformed from granular to rod-shaped with an increase in temperature. TEM images revealed the diameter of sample prepared at 120 degrees C is about 10-50nm. HRTEM showed that crystals prepared at 120 degrees C grew along {111} surfaces. The PL results indicated that samples prepared at 180 degrees C without EDTA have the strongest luminescence property. (C) 2016 Optical Society of America
卷号:6
期号:4
是否译文:否